Ethylamine → N-Ethyl-5-methyl-1,3,4-thiadiazole-2-methanamine

HRID 1674636Notes

Reaction equation

HRID 1674636 reaction equation

[CH3:1][C:2]1[S:6][C:5]([CH:7]=O)=[N:4][N:3]=1.[CH2:9]([NH2:11])[CH3:10]>C1COCC1>[CH2:9]([NH:11][CH2:7][C:5]1[S:6][C:2]([CH3:1])=[N:3][N:4]=1)[CH3:10]

Participants

4

Reactant 2

HCID 6341Ethylamine

HCID 205105195-Methyl-1,3,4-thiadiazole-2-carbaldehyde

Product 1

HCID 45123404N-Ethyl-5-methyl-1,3,4-thiadiazole-2-methanamine

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

prepared by reaction of 5-methyl-[1,3,4]thiadiazole-2-carbaldehyde with 2M ethylamine in THF.

Sources & evidence

ORD record: ord-c96e22375e8e4bd381b11c90e5b9915b
Source dataset: uspto-grants-2011_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08003654B2

Reaction notes

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