HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-3-[chloro(difluoro)methyl][1,2,4]triazolo[4,3-b]pyridazine → HCID 59149725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-3-[chloro(difluoro)methyl][1,2,4]triazolo[4,3-b]pyridazine | HCID 1489114 | — |
| Reactant | 4-Phenyl-azepane HCl | HCID 24200663 | — |
| Product | HCID 59149725 | HCID 59149725 | 69% |
Reaction Steps
A mixture of 4-phenylazepane hydrochloride and 6-chloro-3-[chloro(difluoro)methyl]-[1,2,4]triazolo[4,3-b]pyridazine was allowed to react by an analogous method to Example 331 to give 3-[chloro(difluoro)methyl]-6-(4-phenylazepan-1-yl)[1,2,4]triazolo[4,3-b]pyridazine in 69% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003649B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-fe1e3deb2e0c4ffc871ee0b7f86f169f |
| Source note | uspto-grants-2011_08 |