HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-butanone → HCID 53396467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-butanone | HCID 11251 | — |
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Product | HCID 53396467 | HCID 53396467 | 80% |
Reaction Steps
3-Methylbutan-2-one (2.5 g, 1 eq.) and dimethylformamide diethylacetal (7.46 mL, 1.5 eq.) were heated at 100° C. for 4 days to give compound 85 as yellow viscous oil in 80% yield., which was used directly without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003659B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-873004a3c87648fea2f6b8b76cad78fa |
| Source note | uspto-grants-2011_08 |