HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 66995933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoro-5-(trifluoromethyl)phenol | HCID 518888 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 66995933 | HCID 66995933 | — |
Reaction Steps
A mixture of 5-(trifluoromethyl)-2-fluorophenol (2.0 g), benzyl bromide (1.45 ml) and potassium carbonate (1.65 g) in dry DMF (20 ml) was stirred at RT overnight. The mixture was quenched with water and the solid filtered and dried, yield 2.20 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003703B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-540823e120f74b9e87c2e5bca072348f |
| Source note | uspto-grants-2011_08 |