HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 18449380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 86619735 | HCID 86619735 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18449380 | HCID 18449380 | — |
Reaction Steps
(±)-tert-Butyl {3-[4-(methylsulfinyl)-1,3-thiazol-2-yl]-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl}acetate from Step D (100 mg, 0.254 mmol) was dissolved in CF3CO2H (3 mL) and CH2Cl2 (3 mL) and the mixture was stirred at ambient temperature for 3 h, then concentrated in vacuo to give the title compound. MS: m/z=338 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003792B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-1f5810060d984d66af8f7d995a8fb42c |
| Source note | uspto-grants-2011_08 |