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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1675784Generated: October 30, 2026

Trifluoroacetic acid → HCID 67337580, compound

https://huagongshe.com/reaction/1675784

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86619737HCID 86619737—
SolventDichloromethaneHCID 6344—
ProductHCID 67337580HCID 67337580—

Reaction Steps

CF3CO2H (1 mL) was added to a solution of tert-butyl (2-oxo-2′,3′,5′,6′-tetrahydrospiro[indole-3,4′-pyran]-1(2H)-yl)acetate from Step B (55.0 mg, 0.173 mmol) in CH2Cl2 (3 mL). After 3 h, the mixture was concentrated in vacuo to give the title compound. MS: m/z=262 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08003792B2
Source datasetuspto-grants-2011_08
ORD IDord-b40aa94eeaf44a99a8310ec6e28878c4
Source noteuspto-grants-2011_08