Isobutyric Acid → HCID 21900164, compound

HRID 1675974Notes

Reaction equation

HRID 1675974 reaction equation
[OH-].[CH2:2]([N+:6]([CH2:15][CH2:16][CH2:17][CH3:18])([CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH2:9][CH3:10])[CH2:3][CH2:4][CH3:5].[C:19]([OH:24])(=[O:23])[CH:20]([CH3:22])[CH3:21]>O>[C:19]([O-:24])(=[O:23])[CH:20]([CH3:22])[CH3:21].[CH2:15]([N+:6]([CH2:2][CH2:3][CH2:4][CH3:5])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:11][CH2:12][CH2:13][CH3:14])[CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 6590Isobutyric AcidHCID 2723671Tetrabutylammonium Hydroxide

Product 1

HCID 21900164HCID 21900164, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 40 wt % solution of tetrabutylammonium hydroxide in water (250 mL, 99 g, 382 mmol), water (300 mL) and isobutyric acid (33.8 g, 382 mmol) was stirred at ambient temperature for 30 min. The solvent was removed in vacuo to afford the title compound (5) as a waxy solid, which was used without further purification.

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-4ad69fe421474572af74264d4275e195
Source dataset
uspto-grants-2011_08
Patent number
US08003809B2

Reaction notes

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