HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67351938, compound → HCID 58653690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67351938 | HCID 67351938 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 58653690 | HCID 58653690 | — |
Reaction Steps
A solution of ethyl (2Z)-3-(1H-benzimidazol-1-yl)-3-(4-ethylphenyl)-2-propenoate (60 mg, 187 μmol) in hydrochloric acid (10 mL of a 5N solution) was stirred at room temperature for 72 hours, and then heated at reflux for 6 hours. The solution was cooled to room temperature, and evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=6.63 min, MH+ 294].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-e942d07abbd844eeac4752b0777948fb |
| Source note | uspto-grants-2011_08 |