Diethyl Ether → HCID 11594163, compound

Participants

Reaction Steps

A solution of tert-butyl (3R)-3-(1H-benzimidazol-1-yl)-3-phenylpropanoate (92 mg, 285 μmol) in hydrochloric acid (20 mL of a 5N solution) was stirred at room temperature for 48 hours. The solution was then evaporated in vacuo to give a gum. Trituration of this residue with diethyl ether afforded the title compound, [LCMS (Method B, Mobile Phase I) RT=3.45 min, MH+ 267].

Provenance & Evidence