Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1676040Generated: October 31, 2026

HCID 58653632, compound → HCID 11511224, compound

https://huagongshe.com/reaction/1676040

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58653632HCID 58653632—
SolventHydrochloric AcidHCID 313—
ProductHCID 11511224HCID 11511224—

Reaction Steps

A solution of methyl 3-phenyl-3-(4-{4-[(1,4,5,6-tetrahydro-2-pyrimidinylamino)carbonyl]-1-piperidinyl}-1H-benzimidazol-1-yl)propanoate (17 mg, 24 μmol) in hydrochloric acid (10 mL of a 5N solution) was stirred at room temperature for 48 hours. The solution was evaporated in vacuo, and the residue purified by RP-HPLC to afford the title compound, [LCMS (Method A, Mobile Phase II) RT=3.5 min, MH+ 475].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08003806B2
Source datasetuspto-grants-2011_08
ORD IDord-33ad9f132e3b4a46b31881066cea25e5
Source noteuspto-grants-2011_08