HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178470878, compound → HCID 178512493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178470878 | HCID 178470878 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178512493 | HCID 178512493 | — |
Reaction Steps
A solution of ethyl 3-{5-[(3-{[amino(imino)methyl]amino}benzoyl)amino]-1H-benzimidazol-1-yl}-3-phenylpropanoate (32 mg, 68 μmol) in hydrochloric acid (20 mL of a 5N solution) was stirred at room temperature for 96 hours. The solution was evaporated in vacuo and the residue was purified by RP-HPLC to afford the title compound, [LCMS (Method A, Mobile Phase II) RT=2.99 min, MH+ 443].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-dd77218bd2684ba491dd8fb10172ae62 |
| Source note | uspto-grants-2011_08 |