HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178470877, compound → HCID 178512523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178470877 | HCID 178470877 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178512523 | HCID 178512523 | — |
Reaction Steps
A solution of ethyl 3-{6-[(4-{[amino(imino)methyl]amino}benzoyl)amino]-1H-benzimidazol-1-yl}-3-phenylpropanoate (15 mg, 32 μmol) in hydrochloric acid (20 mL of a 5N solution) was stirred at room temperature for 96 hours. The solution was then evaporated in vacuo, and the residue was purified by RP-HPLC to afford the title compound, [LCMS (Method A, Mobile Phase II) RT=2.86 min, MH+ 443].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-7e8bfd9698ab4630b157cac535e827ea |
| Source note | uspto-grants-2011_08 |