HRID1676090

反应详情

EQUATION

反应方程式

HRID 1676090 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of methyl 3-(1,1′-biphenyl)-4-yl-3-{5-[(phenylsulfonyl)amino]-1H-benzimidazol-1-yl}propanoate (12 mg, 23 μmol) in hydrochloric acid (10 mL of a 5N solution) was stirred at room temperature for 120 hours. The solution was evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=5.04 min, MH+ 498].

WORKUP

后处理

  1. customThe solution was evaporated in vacuo