HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 11688159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 58653638 | HCID 58653638 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 11688159 | HCID 11688159 | — |
Reaction Steps
A solution of 1-(3-ethoxy-3-oxo-1-phenylpropyl)-1H-benzimidazole-5-carboxylic acid (40 mg, 118 μmol) in a mixture of hydrochloric acid (10 mL of a 5N solution) and acetonitrile (6 mL) was stirred at room temperature for 72 hours. The solution was evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=5.26 min, MH+ 311].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-a2947b86450c4a7cb0cc4277d92afdc6 |
| Source note | uspto-grants-2011_08 |