HRID1676091
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 1-(3-ethoxy-3-oxo-1-phenylpropyl)-1H-benzimidazole-5-carboxylic acid (40 mg, 118 μmol) in a mixture of hydrochloric acid (10 mL of a 5N solution) and acetonitrile (6 mL) was stirred at room temperature for 72 hours. The solution was evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=5.26 min, MH+ 311].
WORKUP
后处理
- customThe solution was evaporated in vacuo