HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dietylaminopropin → HCID 67347436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dietylaminopropin | HCID 20010 | — |
| Reactant | HCID 67348108 | HCID 67348108 | — |
| Product | HCID 67347436 | HCID 67347436 | — |
Reaction Steps
Prepared from 4-(2-iodothieno[3,2-b]pyridin-7-yloxy)-2-methylbenzenamine (0.250 g, 0.556 mmol), and N,N-diethylprop-2-yn-1-amine (0.0680 g, 0.612 mmol), according to the procedure for Example 6, Step B. The crude was purified by Biotage 40S (EtOAc). The product was an orange oil (116 mg, 39%). LRMS (ESI pos) m/e 366 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003662B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-b3c0fb8ff8744f3397223cf01e4b0885 |
| Source note | uspto-grants-2011_08 |