Trifluoroacetic acid → HCID 86622851, compound

Participants

Reaction Steps

To a solution of 1.98 g (8.7 mmol) of (R)—N-allyl-2-methyl-succinamic acid tert-butyl ester in 30 ml of DCM are added 3.57 ml (21.8 mmol) of triethylsilane and 8.76 ml (113 mmol) of TFA, and the mixture is stirred for 3 h and then concentrated by co-evaporation with toluene (3×30 ml) to give the solid product.

Provenance & Evidence