HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Morpholine-4-sulfonyl)benzoic acid → HCID 15951135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Morpholine-4-sulfonyl)benzoic acid | HCID 559416 | — |
| Reactant | (S)-(+)-1-(2-Pyrrolidinylmethyl)pyrrolidine | HCID 853152 | — |
| Product | HCID 15951135 | HCID 15951135 | 35.8% |
Reaction Steps
The title compound is prepared from 4-(morpholine-4-sulfonyl)-benzoic acid (407 mg, 1.5 mmol) and (S)(+)-1-(2-pyrrolidinylmethyl)pyrrolidine (CAS 51207-66-0)(193 mg, 1.2 mmol) in a manner substantially similar to Procedure G to provide 175 mg (34%) of the title compound. MS (ES+) 408.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008296B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-fdb941e327e94692910d1ad26f3b0380 |
| Source note | uspto-grants-2011_08 |