HRID1676985

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3614772

1-(1,4-Dioxan-2-yl)-N-methylmethanamine

C6H13NO2

HCID6364545

未命名化合物

结构：CCOC(=O)c1c(S(=O)(=O)Cl)c2cc(Cl)ccc2n1S(=O)(=O)c1ccccc1

HCID22401482

未命名化合物

结构：CCOC(=O)c1c(S(=O)(=O)Cl)c2cc(Br)ccc2n1S(=O)(=O)c1ccccc1

HCID86592455

未命名化合物

PRODUCTS

生成物

结构：CN(CC1COCCO1)S(=O)(=O)c1c(C(N)=O)[nH]c2ccc(Br)cc12

HCID58659663

未命名化合物

PROCEDURE

实验过程

Following the procedures described in Steps D and E of Example 1, replacing in Step D ethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate with ethyl 5-bromo-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate, and methylamine hydrochloride with (±)-N-methyl-N-(1,4-dioxan-2-ylmethyl)amine, the title compound was obtained. Proton NMR for the product was consistent with the titled compound. ESI+ MS: 432.2 [M+H]+.