HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10248012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10049933 | HCID 10049933 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10248012 | HCID 10248012 | — |
Reaction Steps
Through a solution of the product from Example 62, Step B (113 mg, 0.245 mmols) in 20 mL of EtOAc at 0° C. was bubbled HCl gas for 3 minutes. The reaction was sealed, and stirring continued for 45 minutes. The solvent was removed in vacuo to give the titled compound. ESI+ MS: 361 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008295B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-4b5e8708ebad485494866f0d675ae67a |
| Source note | uspto-grants-2011_08 |