HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67373460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 86605458 | HCID 86605458 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67373460 | HCID 67373460 | — |
Reaction Steps
The product from Step A above (1 equivalent) was combined with the product from Step C above (1 equivalent) and triethylamine (3 equivalents) in dichloromethane and stirred at room temperature for 1.5 hours. The reaction was diluted with EtOAc, washed with saturated NaHCO3 and brine and dried over Na2SO4. Concentrating in vacuo gave the titled compound. ESI+ MS: 640 [MH—CH3]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008295B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-9a1ef5dd0b114d778688460dda3c2aaa |
| Source note | uspto-grants-2011_08 |