HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Bromobenzenesulfonyl chloride → HCID 67372575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Bromobenzenesulfonyl chloride | HCID 7396 | — |
| Reactant | HCID 67373781 | HCID 67373781 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 67372575 | HCID 67372575 | — |
Reaction Steps
A solution of the product from Example 89 Step A, was combined with 4-bromobenzenesulfonyl chloride and triethylamine, and stirred at room temperature for 35 minutes. The solvent was removed with a stream of nitrogen to give the titled compound. ESI+ MS: 750 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008295B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-21eeb2b973264ebeaec2e2dc1bc7d738 |
| Source note | uspto-grants-2011_08 |