HRID1677046

反应详情

EQUATION

反应方程式

HRID 1677046 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

tert-Butyl 6-(2-(piperidin-1-yl)ethoxy)-3,4-dihydro-1H-pyrido[4,3-b]indole-2(5H)-carboxylate (1.33 g, 3.32 mmol) was added to HCl in MeOH (reagent 10, 25 ml) at 25° C. under air. The resulting solution was stirred at room temperature for 3 days. The solvent was removed under reduced pressure to afford (1.00 g, 100%) as a yellow gum. Material was used crude.

WORKUP

后处理

  1. customThe solvent was removed under reduced pressure
  2. customto afford (1.00 g, 100%) as a yellow gum