HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → HCID 178519486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | HCID 178471912 | HCID 178471912 | — |
| Solvent | 1,1'-Biphenyl, mixt. with 1,1'-oxybis(benzene) | HCID 24670 | — |
| Product | HCID 178519486 | HCID 178519486 | 64% |
Reaction Steps
A solution of ethyl 2-benzoyl-3-[2-(trifluoromethyl)phenylamino]acrylate (30.5 g, 84.0 mmol) in Dowtherm® (280 mL) was stirred at 260° C. for 11 hours. The reaction solution was returned to room temperature, then added with hexane and recrystallized. The title compound (17.0 g, yield 64%) was obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008306B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-4be2271abe41401688a1a7c8791a7a28 |
| Source note | uspto-grants-2011_08 |