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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1677448생성일: 2026년 10월 25일

3-(Aminosulphonyl)benzeneboronic acid → HCID 59540638, 화합물

https://huagongshe.com/reaction/1677448

반응식

참여 물질

역할이름HCID투입량
반응물3-(Aminosulphonyl)benzeneboronic acidHCID 44119323—
반응물1-(2-Bromo-5H-pyrrolo[2,3-b]pyrazin-7-yl)-2,2-dimethylpropan-1-oneHCID 57829218—
용매Ethyl AcetateHCID 8857—
생성물HCID 59540638HCID 59540638—

반응 단계

3-[7-(2,2-Dimethyl-propionyl)-5H-pyrrolo[2,3-b]pyrazin-2-yl]-benzenesulfonamide was prepared starting from 1-(2-bromo-5H-pyrrolo[2,3-b]pyrazin-7-yl)-2,2-dimethyl-propan-1-one and (3-aminosulfonylphenyl)Boronic Acid following general procedures as described in these Examples. Silica gel chromatography using 20-100% EtOAc in hexanes as eluant provided 60 mg (37%) of a pale yellow solid. MP 275-277° C., M+H=359.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08008298B2
출처 데이터셋uspto-grants-2011_08
ORD IDord-f77e56c40f2d4b919929f1bba60e7fe1
출처 메모uspto-grants-2011_08