HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 59540922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59540962 | HCID 59540962 | — |
| Product | HCID 59540922 | HCID 59540922 | 99% |
Reaction Steps
A solution of 4-benzyloxy-1-methyl-cyclohexanecarboxylic acid (1.71 g, 6.89 mmol) in thionyl chloride (10 ml) was refluxed for 2 hours. The reaction mixture was concentrated on high vacuum giving 1.84 g (99%) of 4-benzyloxy-1-methyl-cyclohexanecarbonyl chloride as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008298B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-27f50381b43b4720a59543a5ccda5790 |
| Source note | uspto-grants-2011_08 |