HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67215725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67215491 | HCID 67215491 | — |
| Product | HCID 67215725 | HCID 67215725 | — |
Reaction Steps
This compound is obtained according to the same process as that described in the preceding example 15 by deprotection of the amine of the compound [6-(tert-butoxycarbonylamino)imidazo[1,5-a]pyridin-3-yl](3-methoxy-4-nitrophenyl)methanone with trifluoroacetic acid. A yellow solid is obtained which is salified in the hydrochloride form. Melting point: 252° C.; 1H NMR (d6-DMSO): 4.01 (3H, s), 7.14 (1H, d), 7.79 (1H, s), 7.87 (1H, d), 7.97-8.01 (2H, m), 8.13 (1H, s), 9.41 (1H, s)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008321B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-5446f919b9e84be4977f2eec13601e07 |
| Source note | uspto-grants-2011_08 |