Hexyl isocyanate → HCID 131729124, compound

HRID 1677651Notes

Reaction equation

HRID 1677651 reaction equation
[Br:1][C:2]1[CH:11]=[CH:10][C:5]2[NH:6][C:7](=[O:9])[S:8][C:4]=2[CH:3]=1.N([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=C=O>O1CCOCC1>[Br:1][C:2]1[CH:11]=[CH:10][C:5]2[NH:6][C:7](=[O:9])[S:8][C:4]=2[CH:3]=1.[CH3:20][CH2:19][CH:18]([C:7]([NH2:6])=[O:9])[CH2:17][CH2:16][CH3:15]

Participants

4

Reactant 2

HCID 75659Hexyl isocyanateHCID 1884446-Bromo-2,3-dihydro-1,3-benzothiazol-2-one

Product 1

HCID 131729124HCID 131729124, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

200 mg (0.869 mmol) of 6-bromo-3H-benzothiazol-2-one were reacted in analogy to Example 1 with 132.7 mg (1.04 mmol) of 1-isocyanatohexane in dioxane at 80° C. Yield: 185 mg (59%), M+H+: 357.1.

Sources & evidence

ORD record
ord-3a65384ff267459d85bcfde798e233fb
Source dataset
uspto-grants-2011_08
Patent number
US08008331B2

Reaction notes

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