HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl isocyanate → HCID 131729124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 6-Bromo-2,3-dihydro-1,3-benzothiazol-2-one | HCID 188444 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131729124 | HCID 131729124 | — |
Reaction Steps
200 mg (0.869 mmol) of 6-bromo-3H-benzothiazol-2-one were reacted in analogy to Example 1 with 132.7 mg (1.04 mmol) of 1-isocyanatohexane in dioxane at 80° C. Yield: 185 mg (59%), M+H+: 357.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008331B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-3a65384ff267459d85bcfde798e233fb |
| Source note | uspto-grants-2011_08 |