Hydrochloric Acid → HCID 67235317, compound

HRID 1677724Notes

Reaction equation

HRID 1677724 reaction equation
[C@@H:1]12[CH2:7][CH2:6][C@@H:5]1[CH2:4][N:3]([CH2:8][CH2:9][CH2:10][O:11][C:12]1[CH:20]=[CH:19][C:15]([C:16]([NH2:18])=[O:17])=[CH:14][CH:13]=1)[CH2:2]2.[ClH:21]>C(O)C>[ClH:21].[C@@H:5]12[CH2:6][CH2:7][C@@H:1]1[CH2:2][N:3]([CH2:8][CH2:9][CH2:10][O:11][C:12]1[CH:13]=[CH:14][C:15]([C:16]([NH2:18])=[O:17])=[CH:19][CH:20]=1)[CH2:4]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 52952792HCID 52952792, compound

Product 1

HCID 67235317HCID 67235317, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product obtained in Step 2 is dissolved in 10 ml of ethanol to which 2 ml of 2N ethereal HCl are added. The product thereby obtained is filtered off, rinsed with ethanol and dried in vacuo.

Workup

  1. additionare added
  2. customThe product thereby obtained
  3. filtrationis filtered off
  4. washrinsed with ethanol
  5. customdried in vacuo

Sources & evidence

ORD record
ord-cbe986a1a6c74f848bf4e0bace1ba389
Source dataset
uspto-grants-2011_08
Patent number
US08008337B2

Reaction notes

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