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HRID1677756

反应详情

EQUATION

反应方程式

HRID 1677756 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(c1ccc(Cl)cc1)C(F)(F)F
HCID703324

1-Chloro-4-(trifluoromethanesulfonyl)benzene

C7H4ClF3O2S

结构：C[C@@H]1CN(c2ccc(S(C)(=O)=O)cc2)CCN1
HCID26597658

(3R)-1-[4-(Methanesulfonyl)phenyl]-3-methylpiperazine

C12H18N2O2S

PRODUCTS

生成物

1
结构：C[C@@H]1CN(c2ccc(S(=O)(=O)C(F)(F)F)cc2)CCN1
HCID11580385

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure of Intermediate 26, but starting from 1-chloro-4-(trifluoromethanesulfonyl)benzene. Purification by flash chromatography (CHCl3/MeOH) gave the title compound as a pale yellow solid. M+(ESI): 309.2. HPLC (Condition A), Rt: 2.3 min (HPLC purity: 99.5%).

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by flash chromatography (CHCl3/MeOH)