HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67373446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11595234 | HCID 11595234 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67373446 | HCID 67373446 | — |
Reaction Steps
Stir [3-(2-amino-phenylsulfanyl)-1H-indol-2-yl]-pyrrolidin-1-yl-methanone (Iz, 60 mg) in Et2O (5 mL) with 1N HCl (1 mL) and collect the precipitate by filtration. Wash the filter cake with Et2O and dry to afford the title compound Iaa (48 mg) as a white solid, mp 154-155° C.; m/z=338 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008340B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-1a2ef2de562e4cd296d04acd98252ae0 |
| Source note | uspto-grants-2011_08 |