HRID1678463

反应详情

EQUATION

反应方程式

HRID 1678463 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

5′-tert-Butoxycarbonylamino-2′-methyl-biphenyl-4-carboxylic acid ethyl ester (6.3 g) was stirred in ethanol (75 ml) and 1M sodium hydroxide (30 ml) at 20 C for 18 h. The mixture was then acidified and the ethanol evaporated. The pale beige solid thus formed was collected by filtration and dried (4.26 g)

WORKUP

后处理

  1. customthe ethanol evaporated
  2. customThe pale beige solid thus formed
  3. filtrationwas collected by filtration
  4. customdried (4.26 g)