HRID1678465
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of {4′-[4-(1,1-dioxo-1lambda*6*-thiomorpholin-4-ylmethyl)-phenylcarbamoyl]-6-methyl-biphenyl-3-yl}-carbamic acid tert-butyl ester (685 mg) in ethanol (25 ml) and 6M HCl (25 ml) was stirred at 20 C for 18 h. The mixture was then basified and the ethanol evaporated. The colourless solid thus formed was collected by filtration and dried (434 mg).
WORKUP
后处理
- customthe ethanol evaporated
- customThe colourless solid thus formed
- filtrationwas collected by filtration
- customdried (434 mg)