HRID1678465

反应详情

EQUATION

反应方程式

HRID 1678465 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of {4′-[4-(1,1-dioxo-1lambda*6*-thiomorpholin-4-ylmethyl)-phenylcarbamoyl]-6-methyl-biphenyl-3-yl}-carbamic acid tert-butyl ester (685 mg) in ethanol (25 ml) and 6M HCl (25 ml) was stirred at 20 C for 18 h. The mixture was then basified and the ethanol evaporated. The colourless solid thus formed was collected by filtration and dried (434 mg).

WORKUP

后处理

  1. customthe ethanol evaporated
  2. customThe colourless solid thus formed
  3. filtrationwas collected by filtration
  4. customdried (434 mg)