HRID1678488

反应详情

EQUATION

反应方程式

HRID 1678488 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 5′-(cyclohexanecarbonyl-amino)-2′-chloro-biphenyl-4-carboxylic acid ethyl ester (200 mg) in ethanol (15 ml) and 1M sodium hydroxide (7.5 ml) was stirred at 20 C for 18 h. The ethanol was then evaporated and the residue acidified. The solid thus formed was collected by filtration and dried (176 mg).

WORKUP

后处理

  1. customThe ethanol was then evaporated
  2. customThe solid thus formed
  3. filtrationwas collected by filtration
  4. customdried (176 mg)