HuagongsheHuagongshe Chemistry Print Report · For research reference only
Divinyl sulfone → HCID 43581170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Divinyl sulfone | HCID 6496 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-(4-Aminophenyl)ethylamine | HCID 72895 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 43581170 | HCID 43581170 | — |
Reaction Steps
A mixture of 4-(2-amino-ethyl)-phenylamine (1 g) and ethenesulfonyl-ethene (0.74 ml) in NMP (2.5 ml) containing triethylamine (1.02 ml) was heated to 110 C for 30 mins. The mixture was then allowed to cool and the solid produced was collected by filtration, washed with ether, and dried, giving the title compound as a pale yellow solid (1.59 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008303B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-3423c9b32d534ddaa779d6c9ae512534 |
| Source note | uspto-grants-2011_08 |