Phenylacetyl chloride → HCID 45110383, compound

HRID 1678613Notes

Reaction equation

HRID 1678613 reaction equation
C1(N[C:8]2[N:9]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[N:10]=[C:11]3[C:16]=2[CH:15]=[CH:14][CH:13]=[CH:12]3)CCCCC1.[C:23]1([CH2:29][C:30](Cl)=[O:31])[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>CCN(CC)CC>[CH:17]1([NH:9][C:30](=[O:31])[CH:29]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[C:8]2[N:9]([C:17]3[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=3)[N:10]=[C:11]3[C:16]=2[CH:15]=[CH:14][CH:13]=[CH:12]3)[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1

Participants

4

Reactant 2

HCID 7679Phenylacetyl chlorideHCID 12318206N-Cyclohexyl-2-phenyl-2H-indazol-3-amine

Product 1

HCID 45110383HCID 45110383, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

In analogy to the procedure described in example 1.2, cyclohexyl-(2-phenyl-2H-indazol-3-yl)-amine (example 1.1) was reacted with phenyl-acetyl chloride (CAS Reg. No. 103-80-0) in the presence of Et3N to give the title compound as yellow foam. MS: m/e=410.1 [M+H+].

Sources & evidence

ORD record
ord-a455edc68daa46dda387b6efd2861498
Source dataset
uspto-grants-2011_08
Patent number
US08008505B2

Reaction notes

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