HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178521903, compound → HCID 178478199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178521903 | HCID 178521903 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178478199 | HCID 178478199 | — |
Reaction Steps
In analogy to the procedure described in example 29.1, [rac]-2-[2-(4-chloro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-2-cyclohexyl-N-[2-fluoro-4-(1H-tetrazol-5-yl)-phenyl]-acetamide (example 58) was reduced using borane-dimethylsulfide complex in THF to give the title compound as brown solid. MS: m/e=502.0 [M+H+]1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008505B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-e46532f455c8484d827447aa92d9822f |
| Source note | uspto-grants-2011_08 |