HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 4-tert-Butyl-N-methyl-2,6-dinitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-tert-Butyl-2,6-dinitrochlorobenzene | HCID 75176 | — |
| Product | 4-tert-Butyl-N-methyl-2,6-dinitroaniline | HCID 617279 | — |
Reaction Steps
Following the above procedure, two grams of 40% aqueous solution of methyl amine was reacted with 2.6 grams of 2,6-dinitro-4-t-butyl-chlorobenzene to give N-methyl-2,6-dinitro-4-t-butylaniline as orange needles melting at 129°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077795 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-5df2be3711724d7dbe255d1a415c0583 |
| Source note | uspto-grants-1978_03 |