Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Pyrrolidone → 2-METHOXY-10-[1-(1-Pyrrolin-2-YL)-2-PYRROLIN-2-YL]PHENOTHIAZINE
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Pyrrolidone | HCID 12025 | — |
| 반응물 | Phosphorus oxychloride | HCID 24813 | — |
| 반응물 | Methyl phenothiazin-2-yl ether | HCID 74490 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | 2-METHOXY-10-[1-(1-Pyrrolin-2-YL)-2-PYRROLIN-2-YL]PHENOTHIAZINE | HCID 12799392 | — |
반응 단계
Reaction of 2-methoxyphenothiazine, 2-pyrrolidinone and phosphorus oxychloride in 1,2-dichloroethane according to the procedure of Example 1 affords 2-METHOXY-10-[1-(1-Pyrrolin-2-YL)-2-PYRROLIN-2-YL]PHENOTHIAZINE free base, m.p. 151°-153° C. (corr.), from isopropyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04077959 |
| 출처 데이터셋 | uspto-grants-1978_03 |
| ORD ID | ord-78ff48b7d7c1464b9bf1c35dc3807ec2 |
| 출처 메모 | uspto-grants-1978_03 |