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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1678871Generated: October 31, 2026

Ethylparaben → HCID 19069386, compound

https://huagongshe.com/reaction/1678871

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylparabenHCID 8434—
ReactantPotassium CarbonateHCID 11430—
Reactant2-ChlorothiazoleHCID 76429—
SolventDimethylformamideHCID 6228—
ProductHCID 19069386HCID 1906938627.8%

Reaction Steps

A mixture of 2-chlorothiazole (2.0 g), ethyl 4-hydroxybenzoate (2.8 g), potassium carbonate powder (3.5 g) and dimethylformamide (30 ml) is stirred at 135°-140° C for 6 hours. The reaction mixture is treated in the same manner as in Example 1. From the eluate of 30% ether-benzene, ethyl 4-(2-thiazolyloxy)benzoate (1.16 g) is obtained. IR νmaxCCl 4 1730, 1280 cm-1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04077968
Source datasetuspto-grants-1978_03
ORD IDord-eff65ec915e3461ca31928c7124aae33
Source noteuspto-grants-1978_03