Glycerol → HCID 20364998, compound

HRID 1678993Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=[O:6].[OH:11][CH2:12][CH:13]([CH2:15]O)[OH:14]>>[OH:14][CH:13]1[CH2:12][O:11][CH:5]([C:4]2[CH:7]=[CH:8][CH:9]=[CH:10][C:3]=2[O:2][CH3:1])[O:6][CH2:15]1

Participants

Reactant 2

HCID 753Glycerol

HCID 86582-Methoxybenzaldehyde

Product 1

HCID 20364998HCID 20364998, compound

Procedure

Using the method of Example 5e, 40.8 g 2-methoxybenzaldehyde and 27.6 g glycerol were reacted to form 5-hydroxy-2-(2-methoxyphenyl)-1,3-dioxane, crude b.p. 150°-155° C/10-5 mm.

Workup

customwere reacted

Sources & evidence

ORD record: ord-89c40aacae5d46d5a23a0629bb7c1d4a
Source dataset: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04077982

Reaction notes

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