3-Methoxybenzaldehyde → HCID 20364865, compound

Participants

Reaction Steps

Using the method of Example 16, 2-benzyloxy-1,3-propane-diol (18.0 g, 0.1 mole), and 3-methoxybenzaldehyde (13.6 g, 0.1 mole) were reacted to give 26.0 g of oil which was distilled at 1 × 10-4 mm to give 20.2 g of product which distilled at a pot temperature of 200°-206° C. nmr analysis of this product indicated it to contain 37% cis-5-benzyloxy-2-(3-methoxyphenyl)-1,3-dioxane.

Provenance & Evidence