HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Phenylmethoxy)-1,3-propanediol → HCID 20364906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | — |
| Reactant | Benzyloxyacetaldehyde diethyl acetal | HCID 4321487 | — |
| Product | HCID 20364906 | HCID 20364906 | — |
Reaction Steps
Using the procedure of Example 47, benzyloxyacetaldehyde diethyl acetal and 2-benzyloxy-1,3-propanediol were reacted to give 5-benzyloxy-2-benzyloxymethyl-1,3-dioxane, nD25 1.5438. The ir spectrum was consistent with the assigned structure. The nmr spectrum indicated 28% cis isomer and 72% trans isomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-0f9d7961629a4f7385a862e25d6cccfc |
| Source note | uspto-grants-1978_03 |