HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzaldehyde → HCID 20364907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzaldehyde | HCID 68009 | — |
| Reactant | HCID 20364996 | HCID 20364996 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20364907 | HCID 20364907 | — |
Reaction Steps
Using the procedure of Example 51, 3-fluorobenzaldehyde and 2-(2-fluorobenzyloxy)-2-methylpropanediol were reacted, using benzene as solvent, to give, after separation by column chromatography, c-5-(2-fluorobenzyloxy)-r-2-(3-fluorophenyl)-5-methyl1,3-dioxane, m.p. 86°-87°, and t-5-(2-fluorobenzyloxy)-r-2-(3-fluorophenyl)-5-methyl-1,3-dioxane, m.p. 83°-84°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-73b0a3ed1df0498ba1b63dd21e79a872 |
| Source note | uspto-grants-1978_03 |