HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarboxaldehyde → HCID 70624710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarboxaldehyde | HCID 7364 | — |
| Reactant | HCID 20364943 | HCID 20364943 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 70624710 | HCID 70624710 | — |
Reaction Steps
Using the procedure of Example 51, thiophene-2-carboxaldehyde and 2-(2-fluorobenzyloxy)-2-methyl-1,3-propanediol were reacted, using benzene as solvent, to give, after separation by column chromatograph, c-5-(2-fluorobenzyloxy)-5-methyl-r-2-thienyl-1,3-dioxane, m.p. 111°-112°, and t-5-(2-fluorobenzyloxy)-5-methyl-r-2-thienyl-1,3-dioxane, m.p. 84°-85°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-70b7c6ae79524a20a5c946ea1504f8c5 |
| Source note | uspto-grants-1978_03 |