反应详情

Using the procedure of Example 51, cyclohexanone and 2benzyloxy-1,3-propanediol were reacted, using benzene as solvent, to give after distillation, 3-benzyloxy-1,5-dioxaspiro[5.5]undecane, b.p. 120°-121°/0.05 mm. The ir spectrum was consistent with the assigned structure.

1. customwere reacted
2. customto give
3. distillationafter distillation, 3-benzyloxy-1,5-dioxaspiro[5.5]undecane, b.p. 120°-121°/0.05 mm