HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → 3-Benzyloxy-1,5-dioxaspiro[5.5]undecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 3-Benzyloxy-1,5-dioxaspiro[5.5]undecane | HCID 20364873 | — |
Reaction Steps
Using the procedure of Example 51, cyclohexanone and 2benzyloxy-1,3-propanediol were reacted, using benzene as solvent, to give after distillation, 3-benzyloxy-1,5-dioxaspiro[5.5]undecane, b.p. 120°-121°/0.05 mm. The ir spectrum was consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04077982 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-f2662b8b570741998c7d42ea957721ac |
| Source note | uspto-grants-1978_03 |