HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178463890, compound → HCID 178463877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178463890 | HCID 178463890 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178463877 | HCID 178463877 | — |
Reaction Steps
4-Hydroxy-2-diethylaminopyrimidin-6-yl acetic acid (4.0 g) was suspended in ethanol (50 ml) and the mixture refluxed for 16 hours. The volatile portion of the mixture was then evaporated under reduced pressure to yield 4-hydroxy-2-diethylamino-6-methyl pyrimidine as a white powder, melting at 135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080326 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-3f7a19b4e9aa45d08b52f63ed0edecf2 |
| Source note | uspto-grants-1978_03 |