HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20362465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 20362475 | HCID 20362475 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20362465 | HCID 20362465 | — |
Reaction Steps
3 g. of the compound prepared in Example 12 is dissolved in hot methanol. The solution is saturated with ammonia. A precipitate is formed and the mixture is cooled by placing in the refrigerator. After filtration and purification, the pure product having a melting point of 235°-238° C. is recovered. This product is identified as 1-methyl-2-(5-carbamoyl-isoxazol-3-yl)-5-nitroimidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04080340 |
| Source dataset | uspto-grants-1978_03 |
| ORD ID | ord-d0f2be22405447b1a9cc1508d70e59e4 |
| Source note | uspto-grants-1978_03 |